MARC ayrıntıları
| 000 -LEADER |
|---|
| fixed length control field |
09040nam a2200301 i 4500 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
131213s2006 enkm b a001 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
0419228004 |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
BAUN |
| Language of cataloging |
eng |
| Transcribing agency |
BAUN |
| Description conventions |
rda |
| 049 ## - LOCAL HOLDINGS (OCLC) |
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| Holding library |
BAUN_MERKEZ |
| 050 04 - LIBRARY OF CONGRESS CALL NUMBER |
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| Classification number |
TA435 |
| Item number |
.A48 2006 |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Aligizaki, Kalliopi K. |
| 245 10 - TITLE STATEMENT |
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| Title |
Pore structure of cement-based materials : |
| Remainder of title |
testing, interpretation and requirements / |
| Statement of responsibility, etc |
Kalliopi K. Aligizaki. |
| 264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
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| Place of production, publication, distribution, manufacture |
Abingdon [England] ; |
| -- |
New York : |
| Name of producer, publisher, distributor, manufacturer |
Taylor and Francis, |
| Date of production, publication, distribution, manufacture, or copyright notice |
2006. |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
xli, 388 pages : |
| Other physical details |
illustrations ; |
| Dimensions |
26 cm. |
| 336 ## - CONTENT TYPE |
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| Source |
rdacontent |
| Content Type Term |
text |
| Content Type Code |
txt |
| 337 ## - MEDIA TYPE |
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| Source |
rdamedia |
| Media Type Term |
unmediated |
| Media Type Code |
unmediated |
| 338 ## - CARRIER TYPE |
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| Source |
rdacarrier |
| Carrier Type Term |
volume |
| Carrier Type Code |
volume |
| 490 1# - SERIES STATEMENT |
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| Series statement |
Modern concrete technology series ; |
| Volume number/sequential designation |
12. |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc |
Includes bibliographical references and index. |
| 505 00 - FORMATTED CONTENTS NOTE |
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| Title |
Preface |
| -- |
Acknowledgements |
| -- |
Conversions |
| -- |
Symbols |
| -- |
Abbreviations |
| -- |
List of figures |
| -- |
List of tables |
| -- |
Chapter 1 INTRODUCTION |
| -- |
1.1 SCOPE OF THE BOOK |
| -- |
1.2 PORES IN CEMENT PASTE |
| -- |
1.2.1 Gel pores |
| -- |
1.2.2 Capillary pores |
| -- |
1.2.3 Hollow-shell pores |
| -- |
1.2.4 Air voids |
| -- |
1.2.5 Pore size ranges |
| -- |
1.3 METHODS FOR CHARACTERIZING PORE STRUCTURE |
| -- |
1.4 DEFINITION OF PORE STRUCTURE PARAMETERS |
| -- |
1.4.1 General pores |
| -- |
1.4.1.1 Porosity |
| -- |
1.4.1.2 Hydraulic radius |
| -- |
1.4.1.3 Specific surface area |
| -- |
1.4.1.4 Threshold diameter |
| -- |
1.4.1.5 Pore size distribution |
| -- |
1.4.1.6 Other parameters |
| -- |
1.4.1.7 Factors affecting the parameters measured |
| -- |
1.4.2. Air voids |
| -- |
1.4.2.1. Total air content |
| -- |
1.4.2.2 Specific surface |
| -- |
1.4.2.3 Spacing factor |
| -- |
References |
| -- |
Chapter 2 SPECIMEN PRETREATMENT |
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2.1 WATER REMOVAL |
| -- |
2.1.1 Drying techniques |
| -- |
2.1.1.1 Oven-drying |
| -- |
2.1.1.2 Vacuum-drying |
| -- |
2.1.1.3 P-drying |
| -- |
2.1.1.4 D-drying |
| -- |
2.1.1.5 Direct freeze-drying |
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2.1.1.6 Indirect freeze-drying |
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2.1.1.7 Desiccant drying |
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2.1.1.8 Critical Point Drying |
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2.1.2 Solvent Replacement |
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2.1.2.1 Ease of penetration |
| -- |
2.1.2.2 Physical and chemical interactions |
| -- |
2.1.3 Comparison of different water removal techniques |
| -- |
2.2 PREPARATION FOR MICROSCOPY |
| -- |
2.2.1 Polished surface |
| -- |
2.2.1.1 Cutting, grinding and polishing |
| -- |
2.2.1.2 Impregnation by epoxy resin |
| -- |
· Dry vacuum impregnation |
| -- |
· Fluorescent liquid replacement |
| -- |
2.2.2 Thin sections |
| -- |
2.2.3 Fractured surface |
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2.2.4 Intrusion alloys |
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References |
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Chapter 3 MERCURY INTRUSION POROSIMETRY |
| -- |
3.1 THEORY AND TESTING PROCEDURE |
| -- |
3.1.1 Instrument description |
| -- |
3.1.2 Testing procedure |
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3.1.2.1 Low pressure |
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3.1.2.2 High pressure |
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3.1.3 Calculation of pore size |
| -- |
3.1.4 Pore size distribution |
| -- |
3.1.5 Specific surface area |
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3.2 PLOTS OBTAINED |
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3.2.1 Cumulative intrusion curve |
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3.2.2 Incremental and differential distribution curve |
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3.2.3 Surface area |
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3.2.4 Range of sizes determined |
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3.3 HYSTERESIS AND ENTRAPMENT OF MERCURY |
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3.3.1 Theories proposed to explain hysteresis |
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3.3.1.1 Ink-bottle pores and trapped mercury |
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3.3.1.2 Contact angle hysteresis |
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3.3.1.3 Pore potential theory |
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3.3.1.4 Surface roughness |
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3.3.1.5 Compression of the solid |
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3.3.2 Entrapment of mercury and second intrusion method |
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3.4 PARAMETERS AFFECTING RESULTS |
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3.4.1 Specimen pretreatment |
| -- |
3.4.2 Specimen size |
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3.4.3 Rate of pressure build-up |
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3.4.4 Contact angle |
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3.4.4.1 Parameters affecting contact angle |
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Cement paste characteristics |
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Pore size |
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Mercury purity |
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Surface roughness |
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3.4.4.2 Determination of contact angle |
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3.4.5 Surface tension of mercury |
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3.4.6 Alteration of pore structure |
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3.4.7 Alternative intrusion liquids |
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3.5 ADVANTAGES AND LIMITATIONS |
| -- |
References |
| -- |
Chapter 4 GAS ADSORPTION |
| -- |
4.1 THEORY AND TESTING PROCEDURE |
| -- |
4.2 ANALYSIS OF DATA |
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4.2.1 Adsorption isotherm |
| -- |
4.2.2 Thickness of adsorbed film |
| -- |
4.2.3 Pore size (Kelvin Equation) |
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4.3 TOTAL PORE VOLUME |
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4.3.1 Dubinin-Radushkevich equation |
| -- |
4.4 PORE SIZE DISTRIBUTION |
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4.4.1 The Barrett-Joyner-Halenda method |
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4.4.2 The Cranston-Inkley method |
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4.4.3 The Modelless method and Micropore (MP) analysis method |
| -- |
a) Modelless method [4.33] |
| -- |
b) Micropore analysis method |
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4.5 SPECIFIC SURFACE |
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4.5.1 The Langmuir theory |
| -- |
4.5.2 The Brunauer-Emmett-Teller (BET) theory |
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4.5.3 The Dubinin-Kaganer equation |
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4.5.4 The Harkins-Jura (HJ) relative method |
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4.5.5 The t-plot |
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4.5.6?The ?s-plot |
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4.6 ADSORPTION HYSTERESIS |
| -- |
4.7 FACTORS AFFECTING THE RESULTS |
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4.7.1 Pretreatment method |
| -- |
4.7.2 Type of adsorbate used |
| -- |
4.7.3 Analysis method used |
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4.8 ADVANTAGES AND LIMITATIONS |
| -- |
References |
| -- |
Chapter 5 PYCNOMETRY AND THERMOPOROMETRY |
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5.1 PYCNOMETRY |
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5.1.1 Liquid pycnometry |
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5.1.1.1 Water absorption |
| -- |
5.1.1.2 Water replacement using an alcohol |
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5.1.2 Gas (Helium) Pycnometry and Helium Flow |
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5.1.2.1 Theoretical aspects |
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5.1.2.2 Helium flow |
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5.1.2.3Determination of surface area and hydraulic radius |
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5.1.2.4 Effect of pretreatment |
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5.1.3 Advantages and limiations |
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5.2 THERMOPOROMETRY |
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5.2.1 Theoretical considerations |
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5.2.2 Experimental procedure |
| -- |
5.2.3 Pore size distribution |
| -- |
5.2.4 Determination of the Surface Area and the Average Radius |
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5.2.5 Applications on cement paste |
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5.2.6 Advantages and limitations |
| -- |
References |
| -- |
Chapter 6 NUCLEAR MAGNETIC RESONANCE |
| -- |
6.1 THEORETICAL ASPECTS |
| Statement of responsibility |
/ FUNDAMENTALS |
| Title |
6.1.1 Single nucleus properties |
| -- |
6.1.2 Magnetization of a group of nuclei (bulk magnetization) |
| -- |
Interactions between nuclei |
| -- |
6.2 NMR EXPERIMENT |
| -- |
6.2.1 Instrumentation |
| -- |
6.2.2 NMR excitation and response |
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6.2.2.1 Free Induction Decay |
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6.2.2.2 Fourier transformation and spectrum |
| -- |
6.2.3 Pulse sequences |
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6.2.3.1 Hahn spin echo pulse sequence |
| -- |
6.2.3.2 Inversion recovery pulse sequence |
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6.2.3.3 Carr-Purcell echo pulse sequence |
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6.3 SPIN RELAXATION |
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6.3.1 Spin-lattice relaxation |
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6.3.2 Spin-spin relaxation |
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6.3.3 Inhomogeneous broadening |
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6.4. PORE SIZE DETERMINATION |
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6.4.1 Magnetic Resonance Relaxation Analysis |
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6.4.1.1 Relaxation inside a single pore |
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6.4.1.2 Relaxation inside a distribution of pore sizes |
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Discrete model |
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Diffusion cell model |
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6.4.1.3 Pore size distribution in cement pastes |
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6.4.2 NMR Cryoporometry |
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6.4.3 NMR imaging |
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6.4.3.1 Strong field gradients |
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6.4.3.2 Fast Imaging methods |
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6.5.3.3 Application to porous materials |
| -- |
6.5 ADVANTAGES AND LIMITATIONS |
| -- |
References |
| -- |
Chapter 7 SMALL ANGLE SCATTERING |
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7.1 THEORETICAL ASPECTS |
| -- |
7.2 EXPERIMENTAL PROCEDURE |
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7.2.1 Small-angle X-ray scattering equipment setup |
| -- |
7.2.2 Small-angle neutron scattering equipment setup |
| -- |
7.2.3 Data collection/Measurement |
| -- |
7.3 PLOTS OBTAINED |
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7.3.1 Guinier's plot |
| -- |
7.3.2 Porod's plot |
| -- |
7.4 RANGE OF SIZES |
| -- |
7.5 APPLICATIONS TO CEMENT PASTES |
| -- |
7.5.1 Guinier plot |
| -- |
7.5.2 Porod plot |
| -- |
7.5.3 Scattering contrast |
| -- |
7.5.4 Surface area |
| -- |
7.5.5 Structure of cement paste |
| -- |
7.5.6 Fractal dimension |
| -- |
7.5.7 Factors affecting the results |
| -- |
7.5 ADVANTAGES AND LIMITATIONS |
| -- |
References |
| -- |
Chapter 8 MICROSCOPIC TECHNIQUES AND STEREOLOGY |
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8.1 OPTICAL MICROSCOPY |
| -- |
8.1.1 Types of Microscopes |
| -- |
8.1.2 Characteristics of the microscope |
| -- |
8.2 SCANNING ELECTRON MICROSCOPY |
| -- |
8.2.1 Design and physical basis of operation |
| -- |
8.2.2 The Performance and characteristics of the SEM |
| -- |
8.2.3 Electron-Specimen Interactions and principal images |
| -- |
8.2.3.1 Secondary electrons |
| -- |
8.2.3.2 Backscattered electrons (BSE) |
| -- |
8.2.4 Environmental (scanning) electron microscopy |
| -- |
8.2.5 Transmission electron microscope |
| -- |
8.3 SCANNING ACOUSTIC MICROSCOPY |
| -- |
8.4 IMAGE ANALYSIS |
| -- |
8.4.1 Image analysis steps |
| -- |
8.5 STEREOLOGY |
| -- |
8.5.1 Point Counting |
| -- |
8.5.2 Lineal Analysis |
| -- |
8.5.2.1 Pore volume |
| -- |
8.5.2.2 Pore size distribution |
| -- |
8.5.3 Section Analysis |
| -- |
8.5.3.1 Pore volume |
| -- |
8.5.3.2 Pore size distribution from section diameters |
| -- |
8.5.3.3 Pore size distribution from section areas |
| -- |
8.5.4 Comparison of stereological methods |
| -- |
8.5.4.1 Comparison for pore volume |
| -- |
8.5.4.2 Comparison for pore size distribution |
| -- |
8.6 APPLICATION OF MICROSCOPIC TECHNIQUES TO CEMENT PASTE |
| -- |
MICROSTRUCTURE ANALYSIS |
| -- |
8.7 AIR VOIDS ANALYSIS USING OPTICAL MICROSCOPY |
| -- |
8.7.1 Factors affecting results |
| -- |
8.7.2 Different mathematical parameters |
| -- |
8.7.3 Image analysis of air voids |
| -- |
8.7.4 Section analysis used for air volume |
| -- |
8.7.5 Air void distribution |
| -- |
References |
| -- |
Chapter 9 COMPARISON OF RESULTS BY VARIOUS METHODS (Not final) |
| -- |
9.1 COMPARISON WITH MIP RESULTS |
| -- |
9.1.1 Nitrogen Adsorption |
| -- |
Effect of pretreatment |
| -- |
Reasons of differences |
| -- |
9.1.2 Helium pycnometry |
| -- |
9.1.3 Alcohol Exchange |
| -- |
Water |
| -- |
9.1.4 NMR vs. MIP and Nitrogen Sorption |
| -- |
9.1.5. Small Angle X-Ray Scattering |
| -- |
9.2 COMPARISON WITH NITROGEN ADSORPTION |
| -- |
9.2.1 Helium Pycnometry |
| -- |
9.2.2 Water Sorption |
| -- |
9.2.3 SAXS Vs. Nitrogen Adsorption And Drying |
| -- |
9.3 COMPARISON WITH REPLACEMENT TECHNIQUES |
| -- |
9.3.1 Helium Pycnometry Vs. Methanol Sorption |
| -- |
9.3.2 Alcohol Exchange Vs. Water Saturation |
| -- |
9.3.3 Evaporable Water Vs. Rewetting |
| -- |
9.3.4 Neutron scattering vs. water evaporation |
| -- |
9.3.5 SAXS vs. water sorption |
| -- |
9.4 COMPARISON WITH MICROSCOPY TECHNIQUES |
| -- |
Image analysis using BSE |
| -- |
9.1.6 MIP vs. SEM |
| -- |
MIP vs OM |
| -- |
MIP vs. image analysis by SEM |
| -- |
Pore size distribution |
| -- |
Image analysis vs. |
|
|---|
| Title |
methanol adsorption |
| -- |
References |
| -- |
CONCLUSIONS |
| -- |
Standards |
| -- |
Glossary of terms |
| -- |
Index of terms |
| -- |
Author index |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name as entry element |
Cement |
| General subdivision |
Testing. |
|
|---|
| Topical term or geographic name as entry element |
Porosity. |
| 830 #0 - SERIES ADDED ENTRY--UNIFORM TITLE |
|---|
| 9 (RLIN) |
108345 |
| Uniform title |
Modern concrete technology series (E. & F.N. Spon) |
| 900 ## - EQUIVALENCE OR CROSS-REFERENCE-PERSONAL NAME [LOCAL, CANADA] |
|---|
| Personal Name |
35557 |
|
|---|
| Numeration |
satın |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
|---|
| Source of classification or shelving scheme |
Library of Congress Classification |
| Koha item type |
Kitap |
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