TY - BOOK AU - Cornelis,Rita TI - Handbook of elemental speciation: techniques and methodology SN - 0471492140 AV - QD75.3 .H36 2003 PY - 2003///-] CY - Chichester, West Sussex, England, Hoboken, NJ PB - Wiley KW - Speciation (Chemistry) KW - Technique KW - Methodology KW - Environmental chemistry N1 - Includes bibliographical references and index; 2; Sampling: Collection, Storage; 7 --; 2.1; Sampling: Collection, Processing and Storage of Environmental Samples; 7 --; 2.2; Sampling of Clinical Samples: Collection and Storage; 23 --; 2.3; Food: Sampling with Special Reference to Legislation, Uncertainty and Fitness for Purpose; 47 --; 2.4; Sampling: Collection, Storage -- Occupational Health; 59 --; 3; Sample Preparation; 73 --; 3.1; Sample Treatment for Speciation Analysis in Biological Samples; 73 --; 3.2; Sample Preparation Techniques for Elemental Speciation Studies; 95 --; 3.3; Sample Preparation -- Fractionation (Sediments, Soils, Aerosols and Fly Ashes); 119 --; 4; Separation Techniques; 147 --; 4.1; Liquid Chromatography; 147 --; 4.2; Gas Chromatography and Other Gas Based Methods; 163 --; 4.3; Capillary Electrophoresis in Speciation Analysis; 201 --; 4.4; Gel Electrophoresis for Speciation Purposes; 224 --; 5; Detection; 241 --; 5.1; Atomic Absorption and Atomic Emission Spectrometry; 241 --; 5.2; Flow Injection Atomic Spectrometry for Speciation; 261 --; 5.3; Detection by ICP-Mass Spectrometry; 281 --; 5.4; Plasma Source Time-of-flight Mass Spectrometry: a Powerful Tool for Elemental Speciation; 313 --; 5.5; Glow Discharge Plasmas as Tunable Sources for Elemental Speciation; 334 --; 5.6; Electrospray Methods for Elemental Speciation; 356 --; 5.7; Elemental Speciation by Inductively Coupled Plasma-Mass Spectrometry with High Resolution Instruments; 378 --; 5.8; On-line Elemental Speciation with Functionalised Fused Silica Capillaries in Combination with DIN-ICP-MS; 417 --; 5.9; Speciation Analysis by Electrochemical Methods; 427 --; 5.10; Future Instrumental Development for Speciation; 461 --; 5.11; Biosensors for Monitoring of Metal Ions; 471 --; 5.12; Possibilities Offered by Radiotracers for Method Development in Elemental Speciation Analysis and for Metabolic and Environmentally Related Speciation Studies; 484 --; 6; Direct Speciation of Solids; 505 --; 6.1; Characterization of Individual Aerosol Particles with Special Reference to Speciation Techniques; 505 --; 6.2; Direct Speciation of Solids: X-ray Absorption Fine Structure Spectroscopy for Species Analysis in Solid Samples; 526 --; 7; Calibration; 547 --; 7.1; Calibration in Elemental Speciation Analysis; 547 --; 7.2; Reference Materials; 563 --; 8; Screening Methods for Semiquantitative Speciation Analysis; 591 --; 9; Risk Assessments/Regulations; 605 --; 9.1; Environmental Risk Assessment and the Bioavailability of Elemental Species; 605 --; 9.2; Speciation and Legislation; 629 ER -